1C76
STAPHYLOKINASE (SAK) MONOMER
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 298 |
Detector technology | IMAGE PLATE |
Collection date | 1999-11-28 |
Detector | MARRESEARCH |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 43.920, 59.840, 102.880 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.250 |
R-factor | 0.216 |
Rwork | 0.201 |
R-free | 0.27300 |
RMSD bond length | 0.020 |
RMSD bond angle | 2.010 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.9) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.350 |
High resolution limit [Å] | 2.250 | 2.250 |
Rmerge | 0.043 | 0.182 |
Number of reflections | 6589 | |
<I/σ(I)> | 12.8 | |
Completeness [%] | 97.8 | 97.6 |
Redundancy | 4.4 | 4.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | PEG 8000, pH 8.0, vapor diffusion/hanging drop, temperature 293K |