1AI1

HIV-1 V3 LOOP MIMIC

Experimental procedure

Temperature [K]	287
Detector technology	IMAGE PLATE
Collection date	1995-08
Detector	MARRESEARCH
Spacegroup name	C 2 2 21
格子定数 [Å]	89.930, 154.430, 121.460
格子定数 [度]	90.00, 90.00, 90.00

精密化法

残基	12.000 - 2.800
R因子	0.22
Rwork	0.220
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	1acy
結合長の平均二乗偏差(RMSD) [Å]	0.015 *
結合角の平均二乗偏差(RMSD) [度]	2.000 *
Data reduction software	MOSFLM
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Quality characteristics

	Overall	Outer shell
分解能 [Å] (低)		2.900
分解能 [Å] (高)	2.800	2.800
Rmerge_l_obs	0.080 *
Total number of observations	50028 *
独立反射数	19192
完全性 [%]	92.0	90

結晶化条件

結晶ID	方法	pH	温度	溶液条件
1	Vapor diffusion, sitting drop *	6.5	22 *	pH 6.5

文献の結晶化試薬

ID	結晶ID	溶液	試薬名	濃度 (単位) (単位)	詳細
1	1	drop	sodium potassium phosphate	1.4-1.8 (M)
2	1	drop	Fab	15 (mg/ml)