1ZYE
Crystal structure analysis of Bovine Mitochondrial Peroxiredoxin III
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM14 |
Synchrotron site | ESRF |
Beamline | BM14 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2004-12-13 |
Detector | MARRESEARCH |
Wavelength(s) | 0.9790 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 300.995, 80.679, 124.295 |
Unit cell angles | 90.00, 112.76, 90.00 |
Refinement procedure
Resolution | 35.000 - 3.300 |
R-factor | 0.22819 |
Rwork | 0.226 |
R-free | 0.26486 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB code 1qmv |
RMSD bond length | 0.016 |
RMSD bond angle | 1.586 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((TRUNCATE)) |
Phasing software | PHASER |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.000 | 3.500 |
High resolution limit [Å] | 3.300 | 3.300 |
Rmerge | 0.122 | 0.507 |
Number of reflections | 41825 | |
<I/σ(I)> | 5.1 | 1.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 7.5 | 7.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.2 | 289 | ammonium sulfate, isopropanol, pH 7.2, VAPOR DIFFUSION, SITTING DROP, temperature 289.0K |