1ZNI
INSULIN
Experimental procedure
| Spacegroup name | H 3 |
| Unit cell lengths | 80.700, 80.700, 37.600 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 40.000 - 1.498 |
| Rwork | 0.178 |
| RMSD bond length | 0.023 |
| RMSD bond angle | 0.042 |
| Refinement software | REFMAC |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Batch method * | 5 * | Harding, M.M., (1966) J. Mol. Biol., 16, 212. * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | insulin | 0.1g | |
| 2 | 1 | 1 | hydrochloric acid | 0.04 (M) | |
| 3 | 1 | 1 | zinc sulphate | 0.072 (M) | |
| 4 | 1 | 1 | trisodium citrate | 0.2 (M) | |
| 5 | 1 | 1 | 0.6g | ||
| 6 | 1 | 1 | 0.75 (M) | ||
| 7 | 1 | 1 | hydrochloric acid | 0.1 (M) |
