1ZKR
Crystal structure of the major cat allergen Fel d 1 (1+2)
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | MAX II BEAMLINE I711 |
| Synchrotron site | MAX II |
| Beamline | I711 |
| Temperature [K] | 110 |
| Detector technology | CCD |
| Collection date | 2004-10-02 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.087 |
| Spacegroup name | P 1 |
| Unit cell lengths | 38.588, 42.996, 48.906 |
| Unit cell angles | 70.80, 80.56, 81.53 |
Refinement procedure
| Resolution | 36.510 - 1.640 |
| R-factor | 0.19224 |
| Rwork | 0.191 |
| R-free | 0.21994 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.021 |
| RMSD bond angle | 1.967 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 22.5% PEG3350, 0.5 M CaCl2, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
