1ZII

GCN4-LEUCINE ZIPPER CORE MUTANT ASN16ABA IN THE DIMERIC STATE

Experimental procedure

Source type	SEALED TUBE
Detector technology	IMAGE PLATE
Collection date	1991
Detector	RIGAKU RAXIS
Spacegroup name	C 1 2 1
Unit cell lengths	101.870, 30.350, 21.800
Unit cell angles	90.00, 95.19, 90.00

Refinement procedure

Resolution	6.000 - 1.800
R-factor	0.182 *
Rwork	0.182
RMSD bond length	0.020
RMSD bond angle	2.900
Data reduction software	R-AXIS
Data scaling software	R-AXIS
Refinement software	TNT

Data quality characteristics

	Overall
High resolution limit [Å]	1.800 *
Rmerge	0.034
Total number of observations	14869 *
Number of reflections	5897
Completeness [%]	94.0
Redundancy	2.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	peptide	20 (mg/ml)
2	1	reservoir	potassium phosphate	25 (mM)
3	1	reservoir		0.3 (M)
4	1	reservoir	PEG1450	9 (%)