1YW9

h-MetAP2 complexed with A849519

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	110
Wavelength(s)	1.54
Spacegroup name	C 2 2 21
Unit cell lengths	89.956, 98.801, 100.904
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	18.680 - 1.640
Rwork	0.225
R-free	0.24600
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Refinement software	CNX (2002)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	1.640
Number of reflections	51755
<I/σ(I)>	26.4
Completeness [%]	93.7
Redundancy	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1