1YW8

h-MetAP2 complexed with A751277

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	110
Wavelength(s)	1.54
Spacegroup name	C 2 2 21
Unit cell lengths	89.527, 99.225, 101.191
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	19.980 - 2.650
Rwork	0.204
R-free	0.27300
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNX (2002)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.650
Number of reflections	12990
<I/σ(I)>	21
Completeness [%]	97.0
Redundancy	4.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1