1YUP
Reindeer beta-lactoglobulin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Wavelength(s) | 1.731140 |
| Spacegroup name | P 1 |
| Unit cell lengths | 52.240, 94.140, 64.150 |
| Unit cell angles | 90.00, 105.76, 90.00 |
Refinement procedure
| Resolution | 19.960 - 2.100 |
| R-factor | 0.23879 |
| Rwork | 0.235 |
| R-free | 0.31144 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1beb |
| RMSD bond length | 0.014 |
| RMSD bond angle | 1.558 |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.1.24) |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 6 | 277 | 2.6M Na malonate, pH 6.0, VAPOR DIFFUSION, SITTING DROP, temperature 277K |
