1YUH

FAB FRAGMENT

Experimental procedure

Detector technology	AREA DETECTOR
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	81.200, 86.900, 131.100
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 3.000
R-factor	0.19
Rwork	0.190
RMSD bond length	0.017
RMSD bond angle	4.080
Data reduction software	XENGEN
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	3.000 *
Rmerge	0.047
Number of reflections	16470
Completeness [%]	70.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.52 *		Yuhasz, S.C., (1989) J.Mol.Biol., 209, 319. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	Fab	22 (mg/ml)
2	1	reservoir	sodium phosphate	20 (mM)
3	1	reservoir	PEG3400	32 (%(w/v))