1YU3
Major Tropism Determinant I1 Variant
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Wavelength(s) | 1.5479 |
| Spacegroup name | P 63 |
| Unit cell lengths | 92.308, 92.308, 102.290 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 25.940 - 2.520 |
| R-factor | 0.17254 |
| Rwork | 0.170 |
| R-free | 0.21304 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1yu0 |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.013 |
| Data reduction software | HKL-2000 |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.610 |
| High resolution limit [Å] | 2.520 | 2.520 |
| Number of reflections | 16724 | |
| Completeness [%] | 99.9 | 99.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 298 | Isopropanol, Sodium Citrate, HEPES, pH 7.5, VAPOR DIFFUSION, temperature 298K |
