1YQM

Catalytically inactive human 8-oxoguanine glycosylase crosslinked to 7-deazaguanine containing DNA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	NSLS BEAMLINE X4A
Synchrotron site	NSLS
Beamline	X4A
Detector technology	CCD
Collection date	2003-03-08
Detector	ADSC QUANTUM 4
Wavelength(s)	0.979
Spacegroup name	P 65 2 2
Unit cell lengths	92.508, 92.508, 210.649
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	37.290 - 2.500
R-factor	0.212
Rwork	0.212
R-free	0.26100
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.200
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.010	2.590
High resolution limit [Å]	2.500	2.500
Number of reflections	17250
Completeness [%]	89.8	76.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1