1YQK

Human 8-oxoguanine glycosylase crosslinked with guanine containing DNA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CHESS BEAMLINE A1
Synchrotron site	CHESS
Beamline	A1
Detector technology	CCD
Collection date	2003-01-17
Detector	ADSC QUANTUM 4
Wavelength(s)	0.936
Spacegroup name	P 65 2 2
Unit cell lengths	92.358, 92.358, 211.312
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	29.060 - 2.500
R-factor	0.235
Rwork	0.235
R-free	0.27000
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.300
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	29.060	2.590
High resolution limit [Å]	2.500	2.500
Number of reflections	17212
Completeness [%]	89.6	79.5

Crystallization Conditions

crystal ID	method	pH	temperature	details
1