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1YQD

Sinapyl Alcohol Dehydrogenase complexed with NADP+

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSSRL BEAMLINE BL9-2
Synchrotron siteSSRL
BeamlineBL9-2
Temperature [K]298
Detector technologyCCD
Collection date2002-04-25
DetectorADSC QUANTUM 4
Wavelength(s)1.2822
Spacegroup nameP 21 21 2
Unit cell lengths76.477, 137.796, 69.523
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution38.320 - 1.650
R-factor0.195
Rwork0.195
R-free0.21300
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)unrefined structure of the same protein solved by MAD
RMSD bond length0.011
RMSD bond angle1.600
Data reduction softwareHKL-2000
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]38.3001.700
High resolution limit [Å]1.6501.650
Number of reflections83917
Completeness [%]94.189.3
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP6298polyethylene glycol monomethyl ether 5000, polyethylene glycol 400, MOPSO, DTT, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 298K

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