1YNZ
SH3 domain of yeast Pin3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | BESSY BEAMLINE 14.1 |
| Synchrotron site | BESSY |
| Beamline | 14.1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-09-01 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.9537 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 88.550, 26.940, 23.770 |
| Unit cell angles | 90.00, 102.76, 90.00 |
Refinement procedure
| Resolution | 15.000 - 2.200 |
| R-factor | 0.21235 |
| Rwork | 0.211 |
| R-free | 0.24227 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.346 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 2.300 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 2805 | |
| <I/σ(I)> | 10.1 | 4.6 |
| Completeness [%] | 96.8 | 98.6 |
| Redundancy | 3 | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
