1YHJ
Crystal Structure of Pyridoxal Kinase in Complex with Roscovitine and Derivatives
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 113 |
Detector technology | IMAGE PLATE |
Detector | RIGAKU |
Wavelength(s) | 1.5418 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 103.173, 103.173, 58.538 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.800 |
Rwork | 0.226 |
R-free | 0.28500 |
Structure solution method | MOLECULAR REPLACEMENT |
Data reduction software | CrystalClear ((MSC/RIGAKU)) |
Data scaling software | CrystalClear ((MSC/RIGAKU)) |
Phasing software | AMoRE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Rmerge | 0.105 | 0.267 |
Number of reflections | 9070 | |
Completeness [%] | 99.6 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.4 | 300 | 1.4M ammonium sulfate, 100mM KH2PO4-K2HPO4, pH 6.4, VAPOR DIFFUSION, HANGING DROP, temperature 300K |