1YET

GELDANAMYCIN BOUND TO THE HSP90 GELDANAMYCIN-BINDING DOMAIN

Experimental procedure

Detector technology	IMAGE PLATE
Collection date	1997-01-03
Detector	RIGAKU
Spacegroup name	P 1 21 1
Unit cell lengths	53.700, 44.300, 54.650
Unit cell angles	90.00, 116.10, 90.00

Refinement procedure

Resolution	6.000 - 1.900
R-factor	0.193
Rwork	0.193
RMSD bond length	0.007
RMSD bond angle	1.442
Data reduction software	HKL
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	1.900 *
Rmerge	0.025
Total number of observations	86335 *
Number of reflections	16906
Completeness [%]	92.2
Redundancy	5.1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	Tris-HCl	0.1 (M)
2	1	1	sodium acetate	0.2 (M)
3	1	1	PEG4000	33 (%(w/v))