1YDX
Crystal structure of Type-I restriction-modification system S subunit from M. genitalium
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID29 |
Synchrotron site | ESRF |
Beamline | ID29 |
Wavelength(s) | 0.97935, 0.97950, 0.97565, 0.97930 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 76.601, 76.601, 174.847 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 2.300 |
R-factor | 0.1988 |
Rwork | 0.197 |
R-free | 0.23126 |
Structure solution method | MAD |
RMSD bond length | 0.020 |
RMSD bond angle | 1.541 |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.000 | 2.320 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.083 | 0.620 |
Number of reflections | 30905 | |
<I/σ(I)> | 16.7 | 2.5 |
Completeness [%] | 99.6 | 98.8 |
Redundancy | 7 | 6.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |