1YD8

COMPLEX OF HUMAN GGA3 GAT DOMAIN AND UBIQUITIN

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Temperature [K]	95
Detector technology	IMAGE PLATE
Collection date	2004-07-28
Detector	RIGAKU RAXIS IV
Spacegroup name	C 1 2 1
Unit cell lengths	47.886, 97.293, 66.459
Unit cell angles	90.00, 90.03, 90.00

Refinement procedure

Resolution	26.850 - 2.800
R-factor	0.221
Rwork	0.221
R-free	0.29700
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	MODIFIED GGA1 GAT DOMAIN MADE WITH MODELER
RMSD bond length	0.009
RMSD bond angle	1.300
Data scaling software	SCALEPACK
Phasing software	COMO
Refinement software	CNS

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	26.850	2.900
High resolution limit [Å]	2.800	2.800
Rmerge	0.080	0.361
Number of reflections	5999
<I/σ(I)>	12.1	2.6
Completeness [%]	95.4	81.1
Redundancy	2.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1