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1Y95

HIV-1 Dis(Mal) Duplex Pb-Soaked

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsENRAF-NONIUS
Temperature [K]293
Detector technologyIMAGE PLATE
Collection date1999-04-23
DetectorMACSCIENCE
Wavelength(s)1.54
Spacegroup nameP 31 2 1
Unit cell lengths59.200, 59.200, 65.800
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution7.970 - 2.800
R-factor0.226
Rwork0.226
R-free0.25300
Structure solution methodFOURIER SYNTHESIS
RMSD bond length0.004
RMSD bond angle0.800
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]8.0002.970
High resolution limit [Å]2.8002.800
Number of reflections3213
<I/σ(I)>12.63.2
Completeness [%]96.394.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7310MPD, spermine, KCl, MgCl2, Na Cacodylate, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 310K
Crystallization Reagents
IDcrystal IDsolution IDreagent nameconcentrationdetails
111MPD
1012Na Cacodylate
211spermine
311KCl
411MgCl2
511Na Cacodylate
611H2O
712MPD
812KCl
912MgCl2

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