1Y6S
HIV-1 DIS(Mal) duplex Ba-soaked
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Detector | MACSCIENCE |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 58.010, 58.010, 65.420 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.990 - 2.900 |
R-factor | 0.248 |
Rwork | 0.248 |
R-free | 0.27600 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.004 |
RMSD bond angle | 0.800 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 12.000 | 2.930 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 3323 | |
Completeness [%] | 99.8 | 99 |
Redundancy | 8.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7 | 310 | MPD, spermine, KCl, MgCl2, Na Cacodylate, pH 7.0, VAPOR DIFFUSION, SITTING DROP, temperature 310K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | MPD | ||
10 | 1 | 2 | Na Cacodylate | ||
2 | 1 | 1 | spermine | ||
3 | 1 | 1 | KCl | ||
4 | 1 | 1 | MgCl2 | ||
5 | 1 | 1 | Na Cacodylate | ||
6 | 1 | 1 | H2O | ||
7 | 1 | 2 | MPD | ||
8 | 1 | 2 | KCl | ||
9 | 1 | 2 | MgCl2 |