1Y2O
Structure of N-terminal domain IRSp53/BAIAP2
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX14.2 |
| Synchrotron site | SRS |
| Beamline | PX14.2 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-07-25 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 0.9781, 0.9776, 0.9649 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 49.879, 64.164, 74.586 |
| Unit cell angles | 90.00, 106.18, 90.00 |
Refinement procedure
| Resolution | 47.800 - 2.200 |
| R-factor | 0.23021 |
| Rwork | 0.228 |
| R-free | 0.26683 |
| Structure solution method | MAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.032 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | SOLVE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.800 | 2.320 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Rmerge | 0.056 | 0.192 |
| Number of reflections | 22459 | |
| <I/σ(I)> | 25.9 | 8.4 |
| Completeness [%] | 97.4 | 93.7 |
| Redundancy | 3.9 | 3.7 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
