1Y0U
Crystal Structure of the putative arsenical resistance operon repressor from Archaeoglobus fulgidus
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-BM |
| Synchrotron site | APS |
| Beamline | 19-BM |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-07-21 |
| Detector | SBC-3 |
| Wavelength(s) | 0.97916 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 36.741, 43.244, 61.674 |
| Unit cell angles | 90.00, 96.13, 90.00 |
Refinement procedure
| Resolution | 61.310 - 1.600 |
| R-factor | 0.17331 |
| Rwork | 0.172 |
| R-free | 0.20144 |
| Structure solution method | SAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.122 |
| Data scaling software | HKL-2000 |
| Phasing software | HKL-3000 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 61.310 | 1.660 |
| High resolution limit [Å] | 1.600 | 1.600 |
| Rmerge | 0.072 | 0.286 |
| Number of reflections | 22399 | |
| <I/σ(I)> | 11.1 | 4.1 |
| Completeness [%] | 87.9 | 45.9 |
| Redundancy | 7 | 5.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 295 | PEG 3350, sodium acetate, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
