1XZM
FUSARIUM SOLANI CUTINASE COMPLEX WITH N-UNDECYL O-METHYL CHLORO PHOSPHONATE ESTER
Experimental procedure
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 35.120, 67.360, 37.050 |
| Unit cell angles | 90.00, 93.90, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.750 |
| R-factor | 0.144 |
| Rwork | 0.144 |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.400 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 1.750 * |
| Rmerge | 0.055 |
| Total number of observations | 122231 * |
| Number of reflections | 16563 |
| Completeness [%] | 95.0 |
| Redundancy | 7.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG6000 | 2-20 (%(w/v)) | |
| 2 | 1 | drop | HEPES | 100 (mM) | |
| 3 | 1 | drop | cutinase | 5-15 (mg/ml) | |
| 4 | 1 | drop | n-octyl-beta-D-glucopyranoside | 6 (mM) |
