1XZK
FUSARIUM SOLANI CUTINASE COMPLEX WITH DI(ISOPROPYL)PHOSPHATE
Experimental procedure
| Detector technology | IMAGE PLATE |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 37.200, 94.800, 55.000 |
| Unit cell angles | 90.00, 101.30, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.010 |
| R-factor | 0.161 |
| Rwork | 0.161 |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.850 |
| Data reduction software | MOSFLM |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| High resolution limit [Å] | 2.010 * |
| Rmerge | 0.046 |
| Total number of observations | 52036 * |
| Number of reflections | 22117 |
| Completeness [%] | 90.0 |
| Redundancy | 2.66 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | PEG6000 | 2-20 (%(w/v)) | |
| 2 | 1 | drop | HEPES | 100 (mM) | |
| 3 | 1 | drop | cutinase | 5-15 (mg/ml) | |
| 4 | 1 | drop | n-octyl-beta-D-glucopyranoside | 6 (mM) |
