Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 298 |
| Detector technology | AREA DETECTOR |
| Collection date | 1992-02-29 |
| Detector | SIEMENS HI-STAR |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 46.500, 83.470, 95.460 |
| Unit cell angles | 90.00, 90.01, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.880 |
| Rwork | 0.175 |
| R-free | 0.21400 |
| Structure solution method | MIR |
| Starting model (for MR) | 2BLT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.440 |
| Data reduction software | X-GEN |
| Data scaling software | X-GEN |
| Phasing software | PHASES |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 100.000 | 1.970 |
| High resolution limit [Å] | 1.860 | 1.860 |
| Rmerge | 0.039 | 0.274 |
| Number of reflections | 51415 | |
| <I/σ(I)> | 40.5 | 2.7 |
| Completeness [%] | 0.9 | 0.537 |
| Redundancy | 2.5 | 1.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 298 | PEG 8000, SODIUM CACODYLATE, MgCl2, NaN3, pH 6.5 - 8.5, VAPOR DIFFUSION, temperature 298K |
