1XUK
TRYPSIN-BABIM-SULFATE, PH 5.9
Experimental procedure
Detector technology | IMAGE PLATE |
Detector | RIGAKU |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.800, 58.700, 67.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 * - 1.870* |
R-factor | 0.13 |
Rwork | 0.130 |
R-free | 0.17100 |
RMSD bond length | 0.015 |
RMSD bond angle | 26.300 * |
Data reduction software | MSC |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 1.950 | |
High resolution limit [Å] | 1.870 | |
Rmerge | 0.079 | |
Total number of observations | 43750 * | |
Number of reflections | 12500 | |
Completeness [%] | 63.7 | 33.5 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.9 | SYNTHETIC MOTHER LIQUOR = 75% SATURATED MAGNESIUM SULFATE, 25 % 1.0 M MES ADJUSTED TO PH 5.9; SATURATED IN BABIM, COMPLEX PRODUCED BY SOAKING TRYPSIN-BENZAMIDINE CO-CRYSTAL. |