1XRC

CRYSTAL STRUCTURE OF S-ADENOSYLMETHIONINE SYNTHETASE

Experimental procedure

Spacegroup name	P 62 2 2
Unit cell lengths	128.900, 128.900, 139.800
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 - 3.000
R-factor	0.197
Rwork	0.197
R-free	0.25800
RMSD bond length	0.015
RMSD bond angle	25.600 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
Low resolution limit [Å]	10.000
High resolution limit [Å]	3.000
Rmerge	0.070 *
Total number of observations	107591 *
Number of reflections	13378 *
Completeness [%]	96.8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	potassium phosphate	100 (mM)
2	1	1		10 (mM)
3	1	1	ammonium sulfate	33 (%(v/v))
4	1	1	protein	10 (mg/ml)