1XPS

BOVINE RIBONUCLEASE A (PHOSPHATE-FREE) (93 % HUMIDITY)

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	33.490, 106.200, 30.550
Unit cell angles	90.00, 101.96, 90.00

Refinement procedure

Resolution	10.000 - 1.800
R-factor	0.175
Rwork	0.175
R-free	0.24800
RMSD bond length	0.013
RMSD bond angle	25.500 *
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.038
Total number of observations	43080 *
Number of reflections	14420
Completeness [%]	74.6	51 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7.6 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	protein	12 (mg/ml)
2	1	1	Tris-HCl