1XOI
Human Liver Glycogen Phosphorylase A complexed with Chloroindoloyl glycine amide
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X12B |
| Synchrotron site | NSLS |
| Beamline | X12B |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2000-11-15 |
| Detector | BRANDEIS - B4 |
| Spacegroup name | P 31 |
| Unit cell lengths | 123.906, 123.906, 123.103 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 99.000 - 2.100 |
| Rwork | 0.206 |
| R-free | 0.24890 |
| Structure solution method | AB INITIO PHASING |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | CNS |
| Refinement software | CNS |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 99.000 | 2.140 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Number of reflections | 121683 | |
| Completeness [%] | 98.6 | 94.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6 | 290 | pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 290.0K |
