1XOE

N9 Tern influenza neuraminidase complexed with (2R,4R,5R)-5-(1-Acetylamino-3-methyl-butyl-pyrrolidine-2, 4-dicarobyxylic acid 4-methyl esterdase complexed with

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	100
Detector technology	CCD
Detector	MARRESEARCH
Wavelength(s)	1.54
Spacegroup name	I 4 3 2
Unit cell lengths	180.364, 180.364, 180.364
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	9.990 - 2.200
Rwork	0.265
R-free	0.31500
Structure solution method	FOURIER SYNTHESIS
RMSD bond length	0.007
RMSD bond angle	1.500
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	CNS
Refinement software	CNX (2000)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	10.000	2.340
High resolution limit [Å]	2.200	2.200
Number of reflections	22351
Completeness [%]	93.2	89.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1