1XN4
PUTATIVE MAR1 RIBONUCLEASE FROM LEISHMANIA MAJOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.2.2 |
Synchrotron site | ALS |
Beamline | 8.2.2 |
Detector technology | CCD |
Collection date | 2003-11-13 |
Detector | ADSC QUANTUM 315 |
Spacegroup name | I 4 |
Unit cell lengths | 100.431, 100.431, 44.736 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.860 - 3.800 |
Rwork | 0.313 |
R-free | 0.31200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1x9g |
RMSD bond length | 0.006 |
RMSD bond angle | 0.893 |
Data scaling software | SCALEPACK |
Phasing software | EPMR |
Refinement software | REFMAC (refmac_5.2.0005 24/04/2001) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.940 |
High resolution limit [Å] | 3.800 | 3.800 |
Rmerge | 0.126 | |
Number of reflections | 2294 | |
Completeness [%] | 99.9 | 99.6 |
Redundancy | 3.7 | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.2 | 290 | 16% PEG 8000, 0.1 M K2HPO4, 0.1M MOPS pH7.2, VAPOR DIFFUSION, SITTING DROP, temperature 290K, pH 7.20 |