1XES
Crystal structure of stilbene synthase from Pinus sylvestris
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Detector | ADSC QUANTUM 4 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 54.366, 111.373, 131.695 |
| Unit cell angles | 90.00, 93.05, 90.00 |
Refinement procedure
| Resolution | 19.950 - 1.700 |
| R-factor | 0.202 |
| Rwork | 0.202 |
| R-free | 0.22500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | PDB ID 1CGZ |
| RMSD bond length | 0.005 |
| RMSD bond angle | 1.300 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 19.950 |
| High resolution limit [Å] | 1.700 |
| Number of reflections | 171176 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 3.8 | 292 | PEG 4000, citric acid, pH 3.8, VAPOR DIFFUSION, HANGING DROP, temperature 292K |
