1XAO
Hsp40-Ydj1 dimerization domain
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 22-ID |
| Synchrotron site | APS |
| Beamline | 22-ID |
| Temperature [K] | 200 |
| Detector technology | CCD |
| Collection date | 2004-06-29 |
| Detector | MARRESEARCH |
| Wavelength(s) | 0.97936, 0.97947, 0.97242 |
| Spacegroup name | P 61 |
| Unit cell lengths | 49.631, 49.631, 210.191 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 27.160 - 2.070 |
| R-factor | 0.219 |
| Rwork | 0.219 |
| R-free | 0.25800 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.400 |
| Data scaling software | SCALEPACK |
| Phasing software | SOLVE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 27.160 | 2.130 |
| High resolution limit [Å] | 2.070 | 2.070 |
| Number of reflections | 15669 | |
| Completeness [%] | 100.0 | 67.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 5 | 295 | Sodium Chloride, pH 5.0, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
