1X8S
Structure of the Par-6 PDZ domain with a Pals1 internal ligand
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Collection date | 2003-08-15 |
| Spacegroup name | H 3 |
| Unit cell lengths | 63.122, 63.122, 99.276 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 23.900 - 2.503 |
| R-factor | 0.21712 |
| Rwork | 0.216 |
| R-free | 0.25405 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.948 |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 23.900 |
| High resolution limit [Å] | 2.200 |
| Number of reflections | 5889 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.1 | 288 | PEG 6000, pH 7.1, VAPOR DIFFUSION, HANGING DROP, temperature 288K |
