1X6R
Structure 5: room temperature crystal structure of the truncated pak pilin from Pseudomonas aeruginosa at 1.80A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH2R |
Temperature [K] | 293 |
Detector technology | IMAGE PLATE |
Collection date | 2001-08-10 |
Detector | RIGAKU RAXIS |
Wavelength(s) | 1.54 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 38.042, 38.042, 149.580 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.600 - 1.820 |
R-factor | 0.15115 |
Rwork | 0.150 |
R-free | 0.17744 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1dzo |
RMSD bond length | 0.017 |
RMSD bond angle | 1.618 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.600 | 1.850 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.079 | |
Number of reflections | 10367 | |
<I/σ(I)> | 11.59 | |
Completeness [%] | 76.0 | 76 |
Redundancy | 15.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8.2 | 293 | 60% Ammonium Sulfate, 0.1M Hepes, pH 8.2, VAPOR DIFFUSION, temperature 293K |