1X33
T=3 recombinant capsid of SeMV CP
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2003-01-13 |
| Detector | MARRESEARCH |
| Wavelength(s) | 1.54 |
| Spacegroup name | R 3 |
| Unit cell lengths | 291.315, 291.315, 291.315 |
| Unit cell angles | 61.63, 61.63, 61.63 |
Refinement procedure
| Resolution | 15.000 - 3.600 |
| R-factor | 0.232 |
| Rwork | 0.232 |
| R-free | 0.23400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.300 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | GLRF |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 18.000 | 3.730 |
| High resolution limit [Å] | 3.600 | 3.600 |
| Number of reflections | 191916 | |
| Completeness [%] | 76.0 | 62.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 6% PEG 3350, 0.1M MgCl2, Isopropanol, pH 7.5, VAPOR DIFFUSION, HANGING DROP |
