1WSP
Crystal structure of axin dix domain
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SPRING-8 BEAMLINE BL41XU |
| Synchrotron site | SPring-8 |
| Beamline | BL41XU |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2004-03-10 |
| Detector | MARRESEARCH |
| Spacegroup name | P 61 |
| Unit cell lengths | 92.130, 92.130, 85.540 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 29.170 - 2.900 |
| R-factor | 0.246 |
| Rwork | 0.246 |
| R-free | 0.31100 |
| Structure solution method | SAD |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.100 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | SHARP |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 58.772 | 3.060 |
| High resolution limit [Å] | 2.900 | 2.900 |
| Rmerge | 0.073 | 0.224 |
| Number of reflections | 9237 | |
| <I/σ(I)> | 7.5 | 3.3 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 7.2 | 7.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 7.5 | 283 | PEG8000, pH 7.5, VAPOR DIFFUSION, temperature 283K |
