1WLA
MYOGLOBIN (HORSE HEART) RECOMBINANT WILD-TYPE
Experimental procedure
| Detector technology | IMAGE PLATE |
| Collection date | 1993-12-10 |
| Detector | RIGAKU |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 64.296, 28.966, 35.933 |
| Unit cell angles | 90.00, 107.19, 90.00 |
Refinement procedure
| Resolution | 6.000 - 1.700 |
| R-factor | 0.16 * |
| Rwork | 0.160 |
| RMSD bond length | 0.020 |
| RMSD bond angle | 0.038 |
| Data reduction software | OSCILL |
| Refinement software | PROLSQ |
Data quality characteristics
| Overall | |
| Rmerge | 0.083 |
| Total number of observations | 64359 * |
| Number of reflections | 10426 |
| Completeness [%] | 71.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Vapor diffusion, hanging drop * | 8.4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | drop | protein | 8 (mg/ml) | |
| 2 | 1 | drop | ammonium sulfate | 60-62 (%sat) | |
| 3 | 1 | drop | Tris-HCl | 20 (mM) | |
| 4 | 1 | drop | EDTA | 1 (mM) | |
| 5 | 1 | reservoir | ammonium sulfate | 68-70 (%sat) | |
| 6 | 1 | reservoir | Tris-HCl | 20 (mM) | |
| 7 | 1 | reservoir | EDTA | 1 (mM) |
