1WJX

Crystal sturucture of TT0801 from Thermus thermophilus

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Detector technology	CCD
Collection date	2002-11-06
Detector	RIGAKU JUPITER 210
Wavelength(s)	1.000
Spacegroup name	P 65
Unit cell lengths	74.676, 74.676, 47.038
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	50.000 - 1.700
R-factor	0.224
Rwork	0.224
R-free	0.22900
Structure solution method	MOLECULAR REPLACEMENT
Starting model (for MR)	Thermus SmpB derivative (L88M-I104M).
RMSD bond length	0.004
RMSD bond angle	1.300
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	MOLREP
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	1.760
High resolution limit [Å]	1.700	1.700
Number of reflections	16516
<I/σ(I)>	35.9027
Completeness [%]	100.0	100
Redundancy	10.9662

Crystallization Conditions

crystal ID	method	pH	temperature	details
1