1WHP
ALLERGEN PHL P 2
Experimental procedure
| Source type | ROTATING ANODE |
| Source details | RIGAKU RUH2R |
| Temperature [K] | 290 |
| Detector technology | AREA DETECTOR |
| Collection date | 1995 |
| Detector | SIEMENS |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 39.439, 39.439, 121.877 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 8.000 - 3.000 |
| Rwork | 0.192 |
| Structure solution method | MR |
| Starting model (for MR) | 1who |
| RMSD bond length | 0.007 |
| RMSD bond angle | 0.026 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | X-PLOR |
| Refinement software | PROFFT |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.100 |
| High resolution limit [Å] | 3.000 |
| Rmerge | 0.075 |
| Number of reflections | 2177 |
| Completeness [%] | 96.4 |
| Redundancy | 3.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 4.6 | CRYSTALLIZED FROM 24% PEG 4000 SOLUTION., pH 4.6 |
