1WFX

Crystal Structure of APE0204 from Aeropyrum pernix

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Temperature [K]	100
Detector technology	CCD
Collection date	2004-04-06
Detector	RIGAKU JUPITER 210
Wavelength(s)	0.9789, 0.9791, 0.970
Spacegroup name	H 3 2
Unit cell lengths	102.667, 102.667, 101.489
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	44.070 - 2.800
Rwork	0.220
R-free	0.28600
Structure solution method	MAD
RMSD bond length	0.007
RMSD bond angle	1.400
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	44.280	2.900
High resolution limit [Å]	2.800	2.800
Number of reflections	5217
Completeness [%]	99.9	100

Crystallization Conditions

crystal ID	method	pH	temperature	details
1