1WDJ

Crystal structure of TT1808 from Thermus thermophilus HB8

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Temperature [K]	100
Detector technology	CCD
Collection date	2004-02-07
Detector	RIGAKU JUPITER 210
Wavelength(s)	0.9790, 0.9793, 0.9760, 0.9830
Spacegroup name	P 21 21 21
Unit cell lengths	55.682, 95.172, 99.736
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.040 - 2.000
R-factor	0.189
Rwork	0.189
R-free	0.24100
Structure solution method	MAD
RMSD bond length	0.009
RMSD bond angle	1.500
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	30.000	2.070
High resolution limit [Å]	2.000	2.000
Number of reflections	34418
Completeness [%]	95.0	86.8
Redundancy	3.7

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SMALL TUBES	7.5	293	MPD, EtOH, pH 7.5, SMALL TUBES, temperature 293K