1WD5

Crystal structure of TT1426 from Thermus thermophilus HB8

Experimental procedure

Experimental method	MAD
Source type	SYNCHROTRON
Source details	SPRING-8 BEAMLINE BL26B1
Synchrotron site	SPring-8
Beamline	BL26B1
Temperature [K]	100
Detector technology	CCD
Collection date	2004-04-05
Detector	RIGAKU JUPITER 210
Wavelength(s)	0.97910, 0.97938, 0.97400
Spacegroup name	P 41 21 2
Unit cell lengths	103.970, 103.970, 51.287
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	36.760 - 2.000
R-factor	0.195
Rwork	0.195
R-free	0.22700
Structure solution method	MAD
RMSD bond length	0.009
RMSD bond angle	1.200
Data reduction software	HKL-2000
Data scaling software	SCALEPACK
Phasing software	SOLVE
Refinement software	CNS (1.1)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.080
High resolution limit [Å]	2.000	2.000
Number of reflections	31382
<I/σ(I)>	15.37
Completeness [%]	95.3	67.4
Redundancy	7.38

Crystallization Conditions

crystal ID	method	pH	temperature	details
1