1WC8
The crystal structure of mouse bet3p
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | PAL/PLS BEAMLINE 6B |
| Synchrotron site | PAL/PLS |
| Beamline | 6B |
| Temperature [K] | 193 |
| Wavelength(s) | 0.9728, 0.97942, 0.97175 |
| Spacegroup name | P 43 21 2 |
| Unit cell lengths | 54.246, 54.246, 113.757 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 10.000 - 1.900 |
| R-factor | 0.2171 |
| Rwork | 0.217 |
| R-free | 0.26040 |
| Structure solution method | OTHER |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.596 |
| Data scaling software | SCALEPACK |
| Refinement software | CNS |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 30.000 |
| High resolution limit [Å] | 1.900 |
| Rmerge | 0.040 |
| Number of reflections | 141514 |
| Completeness [%] | 97.7 |
| Redundancy | 10.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.8 | 28% POLYETHYLENE GLYCOL 600, 5% POLYETHYLENE GLYCOL 1000, 10% GLYCEROL, AND 0.1 M MES (PH 5.8) |
