1WA6
The structure of ACC oxidase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2003-10-20 |
Detector | MARRESEARCH |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 70.340, 107.060, 108.380 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.550 |
R-factor | 0.189 |
Rwork | 0.186 |
R-free | 0.23600 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1w9y |
RMSD bond length | 0.034 |
RMSD bond angle | 2.344 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | CNS |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.690 |
High resolution limit [Å] | 2.550 | 2.550 |
Rmerge | 0.050 | 0.400 |
Number of reflections | 12798 | |
<I/σ(I)> | 12.6 | 1.9 |
Completeness [%] | 94.3 | 93.4 |
Redundancy | 8.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7.6 | 1.2 M SODIUM DIHYDROGEN PHOSPHATE, 0.6 M DIPOTASSIUM HYDROGEN PHOSPHATE, 0.3 M LITHIUM SULPHATE, 0.1 M CAPS PH 10.5 |