1W9W

Structure of a beta-1,3-glucan binding CBM6 from Bacillus halodurans in complex with laminarihexaose

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Temperature [K]	113
Spacegroup name	P 43 21 2
Unit cell lengths	61.551, 61.551, 121.711
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.000 - 2.100
R-factor	0.208
Rwork	0.205
R-free	0.26700
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.019
RMSD bond angle	2.166
Phasing software	MOLREP
Refinement software	REFMAC (5.1.24)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.000	2.170
High resolution limit [Å]	2.100	2.100
Rmerge	0.060	0.370
Number of reflections	12975
<I/σ(I)>	17.8	4.4
Completeness [%]	95.5	93.5
Redundancy	5.8	6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1