1W9T
Structure of a beta-1,3-glucan binding CBM6 from Bacillus halodurans in complex with xylobiose
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Temperature [K] | 113 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 1 |
| Unit cell lengths | 30.711, 40.967, 56.039 |
| Unit cell angles | 108.89, 105.87, 90.03 |
Refinement procedure
| Resolution | 20.000 - 1.620 |
| R-factor | 0.121 |
| Rwork | 0.118 |
| R-free | 0.17900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1gmm |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.687 |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.2.0003) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 20.000 | 1.680 |
| High resolution limit [Å] | 1.620 | 1.620 |
| Rmerge | 0.050 | 0.240 |
| Number of reflections | 27417 | |
| <I/σ(I)> | 14.9 | 4.5 |
| Completeness [%] | 91.9 | 84.4 |
| Redundancy | 3.6 | 3.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
