1W9K
Dictyostelium discoideum Myosin II motor domain S456E with bound MgADP-BeFx
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE BM30A |
Synchrotron site | ESRF |
Beamline | BM30A |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-04-30 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 104.704, 179.428, 54.153 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.050 |
R-factor | 0.2 |
Rwork | 0.198 |
R-free | 0.23200 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1mma |
RMSD bond length | 0.011 |
RMSD bond angle | 1.407 |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.100 |
High resolution limit [Å] | 2.000 | 2.050 |
Rmerge | 0.060 | 0.260 |
Number of reflections | 68455 | |
<I/σ(I)> | 24 | 4.3 |
Completeness [%] | 96.0 | 96.2 |
Redundancy | 6.2 | 5.2 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 10% PEG 8000, 50 MM HEPES PH 7, 100 MM NACL, 2 MM DTT, 2 MM NAN3 BY MICROSEEDING |