1W8I
The Structure of gene product af1683 from Archaeoglobus fulgidus.
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 150 |
| Detector technology | CCD |
| Collection date | 2004-04-19 |
| Detector | CUSTOM- SBC2 |
| Wavelength(s) | 0.97967, 0.97954 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 66.730, 66.730, 181.381 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 57.830 - 2.100 |
| R-factor | 0.212 |
| Rwork | 0.211 |
| R-free | 0.22500 |
| Structure solution method | MAD |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.136 |
| Data reduction software | HKL-2000 |
| Phasing software | HKL-3000 |
| Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.180 |
| High resolution limit [Å] | 2.100 | 2.100 |
| Rmerge | 0.070 | 0.600 |
| Number of reflections | 26396 | |
| <I/σ(I)> | 9.8 | 3.5 |
| Completeness [%] | 95.8 | 100 |
| Redundancy | 7.6 | 7.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5.5 | SODIUM CITRATE, PEG 3350, GLYCEROL, pH 5.50 |
